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If you notice the stopper surface deteriorating or if the vial no longer holds vacuum (you don't hear a slight hiss when first puncturing), replace the vial or transfer contents to a fresh sealed container

Charlton A, Garzarella J, Jandeleit-Dahm KA, Jha JCJB

Importantly, the narrative is balanced by acknowledging null findings, such as the study by Shirazi-Beechey et al

Racemic ALA and its biologically active enantiomer, R-ALA, are marketed globally as both therapeutic agents and nutritional supplements in various dosage forms ranging from 100 to 600 mg [25,26]